Syllabus

 

BP110P          PHARMACEUTICAL INORGANIC CHEMISTRY (Practical) 4 Hours / Week       


I                Limit tests for following ions

a)      Limit test for Chlorides and Sulphates

b)      Modified limit test for Chlorides and Sulphates Limit test for Iron

c)      Limit test for Heavy metals Limit test for Lead

d)     Limit test for Arsenic


II              Identification test

a)      Magnesium hydroxide Ferrous sulphate Sodium  Bicarbonate Calcium gluconate Copper sulphate


III            Test for purity

a)      Swelling power of Bentonite

b)      Neutralizing capacity of aluminum hydroxide gel

c)      Determination of potassium iodate and iodine in potassium Iodide


IV      Preparation of inorganic pharmaceuticals

a)      Boric acid

b)      Potash alum

c)      Ferrous sulphate

Recommended Books (Latest Editions)

1.      A.H. Beckett & J.B. Stenlake's, Practical Pharmaceutical Chemistry Vol I & II, Stahlone Press of University of London, 4th edition.

2.      A.I. Vogel, Text Book of Quantitative Inorganic analysis

3.      P. Gundu Rao, Inorganic Pharmaceutical Chemistry, 3rd Edition

4.      M.L Schroff, Inorganic Pharmaceutical Chemistry

5.      Bentley and Driver's Textbook of Pharmaceutical Chemistry

6.      Anand & Chatwal, Inorganic Pharmaceutical Chemistry

7.      Indian Pharmacopoeia


Manual of CHOICE BASED CREDIT SYSTEM for Undergraduate Programme (Bachelor of Pharmacy, B. Pharm.) in PHARMACY Revised Course (Revised 2019) from the academic year 2019-2020

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Experiment No. 8 Neutralizing capacity of aluminum hydroxide gel

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Experiment No. 9 Determination of potassium iodate and iodine in potassium Iodide

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Aim:  Determination of iodine (as KI) – Titration method  Reagents  1. Methyl orange indicator – Dissolve 0.50 g of methyl orange in water and dilute to one litre.  2. Dilute sulphuric acid – approximately 2 N.  3. Bromine water – Saturated aqueous solution. Determine the approximate concentration (mg/ml) by adding (from a burette) a measured volume to a flask containing 5 ml of 10 per cent potassium iodide solution, adding 5 ml of dilute sulphuric acid and titrating the liberated iodine with 0.1 N sodium thiosulphate solution.  4. Sodium sulphite solution – approximately one per cent (m/v).  5. Phenol solution – approximately 5 per cent (m/v).  6. Potassium iodide solution – approximately 10 per cent (m/v).  7. Standard sodium thiosulphate solution – 0.005 N (freshly standardized).  8. Starch solution – 1 per cent (freshly prepared) (m/v).  9. Sodium chloride solution – Dissolve 10 g of sodium chloride in water and make up the volume to 100 ml.  10. Potassium iodide control solution –
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Experiment No. 10 Preparation of inorganic pharmaceuticals - Boric Acid

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